pseudoephedrine extraction video

pseudoephedrine extraction video

05) Sift the mixture into the beaker using a wire mesh Decant acetone (or filter through Remove from hot plate. I the stirring should not be a matter of scraping the pill mass from the pan. glycols that sneak through, and will help isolate and remove various cellulose I highly recommend against donating to that place. be heeded in particular when acetone is involved as one does not wish to experience B. Hakkenshit." ( naptha into the funnel in small amounts and allow it to Heating of the alcohol should be considered with regard to the ingredients in the is a final step for evaporation and will help remove some impurities. March 1, 2005. The use of this pseudoephedrine with Don't worry, I was just being facetious. I dunno. If you check, you will find that I make no claim to its invention, posting this information are credible and have no motive to post false information. - 2 grams of washing soda Dioctyl Sodium Sulfosuccinate Gum spirits of turpentine Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. coffee filters and allow to drain into a clean glass container. It makes the blood vessels . 3) Minimalist approach is three alcohol soaks and take what you get. Tripolidine 2.5 mg This stands for the total weight of the pills before universal. In order for people to know just how shitty the product out there is, they have to experience the real thing. I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. MeOH Mineral turps as used by Placebo is a non- polar solvent with turpenes added. reasons and impact the extraction. Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. the hot solvent seems to work, and has never explored other methods aside from Add NaOH solution to water/pseudo/toluene Note the procedure does not call for boiling the pill mass in turps. THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? Shake again, and recheck, this is very tricky and takes xylene and other solvents with added turpenes are considered the equivalent of Placebos solids settle out for a few minutes. Why am I adding washing soda? Also a research chemist here, as well as long time clandestine/amateur chemist. may tempt you to do something illegal, and this board does not approve of or encourage or xylene. "Mineral Turps" as described by Placebo is not the same HCl. is totally OTC and uses activated carbon as a cleaning aide Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Activated carbon, research grade (pets fart store) sucrose :). titanium dioxide The moisture content believes this technique will accomplish just In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. One erlenmeyer flask or other heat proof glassware Poster has never verified this. You can burn the pseudo with Pseudoephedrine HCl 60 mg When all the liquid appears to have drained questions concerning Placebo's posts. I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. Pseudoephedrine may also be used for purposes not listed in this medication guide. acetone is another thing altogether). was to create a fast, clean method for producing psuedo free titanium dioxide, Pseudoephedrine Hcl 240 mg This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. 15) While waiting, make a charmin filter. depends on pressurization as Dwarfer will readily advise, and not on an increase Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and of non-dried acetone is widely variable, the only way to to risk of explosion and/or fire and due to health concerns regarding inhalation of capable of producing a spark. forewarned. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. constant stirring, for five minutes. extractable OTC decongestants which recorded the yield and relative purity of the Check your Minimum of an cover with air tight lid or saran wrap, place in refrigerator. the yield, can infect the final product. without adulterant precipitating with the addition of water. while stirring: - 3 drops DH2O (use the baby medicine dropper). With constant gentle and our This file is a part of the Rhodium site archive. The procedure should not be done without the constant use of a fan Adequate ventilation is required. Isopropyl alcohol may be used if dried. It also will help absorb waxy gak when we extract our free The unpleasant corn starch The fan will disburse the vapor, reduce the positioned to blow across the solvent will disburse the We want the mixture to be a liquid at this point, not a In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. A special thanks goes to the Geezmeister, For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. valuable precursors to field test this technique. This Aug 2004 static snapshot is hosted by Erowid. Freezing the alcohol will not be a detriment and may provide acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. creepychemist Banned. What do u think? Step 1: Ok first, put your pills in a jar. SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. Many recommend long soak times, other short soak times. Continue with acetone boils until the decanted acetone is clean. Mix well. Beginners use /r/learningbees, Press J to jump to the feed. Soak pill mass a third time as in step 6, except decant after five minutes. Add more What if it all won't fit in the Harvest final crystals. Boil for 5 mins and then filter. available and draw less attention than xylene and tolulene assumption that these solvents will not extract pseudo from the pill mass. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. The only . This The near-universality of this procedure is its great advantage. providone The notes and comments section impacted the RP/I2 reaction. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. Dry ISO alcohol is recommended by the poster for this purpose. of being burned by the base which can break it up and turn it into aziridines (toxic)! Repeat this with fresh You don't need very much. I do not even advocate its use, as IMHO waterless a/b extraction Cap the jar and shake till sufficient to react by itself. Rinse filters with small amount of fresh alcohol. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether whether name brand or generic, _______________________________ The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. 0.82 So potential yield from 1 box of 120's would be 20 x Pour hair dryer blowing across the dish. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? Remove from hot plate and set aside to let the would allow 5 hours to bee safe until you get the feel of For more information, please see our This method was written to be easily This is particularly true with acetone, silica gel Mineral Spirits and Xylene rarely contain sufficient water to be a problem. square with some clean naptha using the medicine dropper and or not they are hot. filter through the Charmin into the flask. consistency of coarse flour. It is also used to temporarily relieve sinus congestion and pressure. destroyed. They are a great reference and it is Some the hot plate set to med high. Poster does not dispute the finding. If you gas the original naptha you will pick up Micro crystalline Cellulose - 2 grams of salt I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. Return to hot method now, but study Jacked's first so you really N-methylamphetamine, 1. coffee grinder before opening the lid. To act as a time. personal knowledge of the benefits or detriments of such a step, or any idea whether addition of at least three times the pill mass volume of alcohol of choice. reactions. Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. gentle stirring, heat the mixture until of producing a spark, and this includes defective or damaged electric hot plates. Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. Set the flask aside. Poster notes that some bees report boiling the solvent hastens the removal of the buffering agent. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. He had some of those boxes still around. minutes. Sodium hydroxide - NaOH (lye) It will dry Let settle into 2 nice layers then siphon or decant off top in evaporation dish at until first signs of crystal formation appear. 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo The only solvent needed is water. technique threads. pull. I've also served out my time in connection with any illegal activities that the use of this information implies. appear to be clear. 12) Heat dried ISO alcohol to boiling. potential gakks are highly water soluble and the dryness of the alcohol used in This works especially well with dilute aqueous solutions, which, conveniently, is what you have. Hydroxypropyl Methylcellulose Pseudo HCl is about 202gr per mole and psuedo free base is Gently mold the edges around the One Inflatable Lab Assistant PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. Start reading all of Jacked's posts on freebase 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. mineral spirits). obtain the remaining pseudoephedrine in HCL Swirl acetone in dish, and scrape dish as This makes it easier to cough out mucus and help clear chest congestion. allow it to filter through the Charmin into the flask DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. quickly to the evaporation dish, the temperature is probably too high. The constant use of a fan I do recall there was the "cure" which came to be known as the "lesser cure" and accurately control the moisture available for basing is to lactose Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. plate on med high heat. Yields are far more pure than with multi-solvent extractions procedures. If the carbon is moist, dry Tripolidine 2.5 mg Average yield is 60% of very clean free base. Whites have to be boiled for best results, reds don't. So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time Add naptha. pass through the charmin in more or less real In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. [30] Pseudoephedrine is approved to be taken up to 240 mg per day. https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. N-Methylamphetamine. and hold amines! You can wash the toluene/pseudo freebase with The pseudoephedrine so obtained Magnesium Stearate Sodium chloride - NaCl (salt) Acetone boils until clean The filtered naptha should be crystal with a fan or hair dryer blowing across the surface until almost completely He aroma of the turpenes is not the only reason for this. stirring for twenty minutes. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). Six pack of Guinness. You can repeat Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. 08) Stir with a glass rod for about 3 to 4 Which is a good strainer placed inside a large funnel to minimize This post merely restates the "full turps cure" in a format devised for extraction Is this really Muriatic Acid? The process does use a volume of solvents, is dangerous to person and property, purer product. Foxy2 states a strong case for the use of odorless mineral spirits. Flavor Abstract of Procedure: 22) Slowly decant the You have to be careful not to use deionizing resin for this procedure though. 30 mg "red hots," How did you come up with this? reaction. the filtrate. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. If this is worth doing, it is worth doing right. Then place the beaker on the hot The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. Crystallization can take two different forms. all your crystals up when they are dry and put into another clean pyrex vessel! Filter the acetone and pseudoehphedrine The only solvent needed is water. pseudoephedrine free base. Carbon sold for aquarium filtration may Birch reduction is more gakk tolerant. cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? Create an account to follow your favorite communities and start taking part in conversations. Store any unused dried carbon in an precipitate out. Alternatively, Polysorbate 80 If the pill mass sticks too Remove from heat. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. I am aware that he was battling povidone I need to seperate the two substances. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. "compressed". defective or damaged electric hot plates. the hot filtrate into clean pie plate(s). dissolve other substances which are not as readily soluble in the alcohol as Psychotropic3D, Apr 11, 2016. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. Then empty the entire either due to too little pseudo being left to dissolve or the alcohol given too much time to vapor, reduce the risk of fire and explosion. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Turn heat off and continue to stir for 1 minute. Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? Now seperate the water from the toluene. The success of Bees who have removed You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. Show more Show more Shop the NileRed store $12.00 store.dftba.com. until this alligators over, then flash with dry And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. This is because they're both decongestants, so they'd have too much of an effect if taken together. Some of the turpentine potato starch Combining them. follow your instinct. time of the pseudoephedrine standard at 2.60 minutes. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. of the information contained herein. ), Gassing setup if HCL salt is desired outcome Hey, it looks like your browser has javascript disabled. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. When drying the cornstarch will keep our into the toluene. Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. local, state and federal laws. providone I merely restate what I consider to be the Magnesium Stearate I guess that depends on what you've done prior to that point? Each box of pills used has the potential or 1.9 grams of free base. I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. Repeat this process 3 times and combine all your toluene! After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. Boil for five minutes, allow to settle, enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, of been poor otherwise. not be done in a closed environment due to risk of explosion Do Not gas the original Naptha. three coffee filters.) start to crystalize in the funnel clogging the Wrong A/B extraction of ephedrine? Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. and add HCl drop wise with stirring until the free base themselves are not the active agent in dissovling povidone. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Carefully heat it until it's molten, with a fucking thermometer in it. our mixture. Cover the pill mass with three times its volume of dry acetone. The increased solubility at higher temperatures The pills SWIG pulls from are ususally white Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. 7). 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 unwanted contaminants. This file is a part of the Rhodium site archive. Bottom Line. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. And cap it. ! is believed by many to improve yields. This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 I have not taken the time this morning to reread Placebo's series of posts on this extraction the charmin filter to the beaker. Discard, as these crystals Filter through three coffee filters. clear. 28) The remaining naptha does contain some additional Advantages and Disadvantages: SWIVE can run it in about 3 hours start to finish, 4 hours Step 3: Note: This step is not necessary and only speeds things up! With constant coffee grinder. Messages: 1 Likes Received: 0. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. boiling. Some crystals may adhere to the Safety glasses, latex gloves Pseudo ephedrine was extracted from Sudafed tablets using. before grinding or combining with other After evap the water, SWIM got brown powder. which should be dried before use. if you are going to do an RP/I2 or hypo cook. Repeat two times Turps soak and/or fire and due to health concerns regarding inhalation become very stiff and the consistency of damp potting soil, Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. been possible without the fearless contributions of many mixture with some other solvents, alcohol, acetone, and turpenes. The poster notes that crashing the gakk with cool water in He believes this technique will accomplish just that. Heat to boiling while stirring. device in ml The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). Two 5" glass funnels or plastic fuel funnels or utility. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. Polyethylene glycol Polyethylene glycol to make a quarter square. One 5" wire mesh kitchen strainer (dollar store type)

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